Chlorosulfamic acid → HCID 86657479, compound

HRID 711869Notes

Reaction equation

HRID 711869 reaction equation
[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([O:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][OH:17])[C:3]=1[C:4]#[N:5].[S:18](Cl)(=[O:21])(=[O:20])[NH2:19]>>[S:18](=[O:21])(=[O:20])([O:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][O:10][C:6]1[CH:7]=[CH:8][CH:9]=[C:2]([NH:1][S:18](=[O:21])(=[O:20])[NH2:19])[C:3]=1[C:4]#[N:5])[NH2:19]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 66746538HCID 66746538, compound

Product 1

HCID 86657479HCID 86657479, compoundYield 20%

Procedure

Prepared as in Example 215a from 2-amino-6-(6-hydroxy-hexyloxy)benzonitrile (Example 240b) and sulfamoyl chloride in 20% yield. MS 393 (MH+).

Sources & evidence

ORD record
ord-87cb7a6e63214b6f8009348938e1aa32
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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