HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dinitrobenzonitrile → 2-(5-(Tert-butyldimethylsilyloxy)pentyloxy)-6-nitrobenzonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dinitrobenzonitrile | HCID 520718 | — |
| Reactant | 5-((Tert-butyldimethylsilyl)oxy)pentan-1-ol | HCID 3614318 | — |
| Product | 2-(5-(Tert-butyldimethylsilyloxy)pentyloxy)-6-nitrobenzonitrile | HCID 66745895 | 46% |
Reaction Steps
Prepared as in Example 215c from 5-(tert-butyldimethyl-silyloxy)pentan-1-ol and 2,6-dinitrobenzonitrile as a pale yellow solid in 46% yield. MS 365 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-1b896d2e5b344e14b0dbf9f8f758fc2f |
| Source note | uspto-grants-2015_11 |