HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → 1-(2-Cyano-3-nitrophenoxy)-2,2,4-trimethylpentan-3-yl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | 2-(3-Hydroxy-2,2,4-trimethylpentyloxy)-6-nitrobenzonitrile | HCID 67399238 | — |
| Product | 1-(2-Cyano-3-nitrophenoxy)-2,2,4-trimethylpentan-3-yl acetate | HCID 67399939 | 50% |
Reaction Steps
Prepared as in Example 231c from 2-(3-hydroxy-2,2,4-trimethylpentyloxy)-6-nitrobenzonitrile (Example 243d) and acetyl chloride in 50% yield. MS 335 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181276B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-baad0992ceb049aa8ecb3a300f48e41c |
| Source note | uspto-grants-2015_11 |