Chlorosulfamic acid → HCID 66746588, compound

HRID 711877Notes

Reaction equation

HRID 711877 reaction equation
[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([O:10][CH2:11][CH2:12][CH2:13][CH2:14][S:15][CH3:16])[C:3]=1[C:4]#[N:5].[S:17](Cl)(=[O:20])(=[O:19])[NH2:18]>>[S:17]([NH:1][C:2]1[CH:9]=[CH:8][CH:7]=[C:6]([O:10][CH2:11][CH2:12][CH2:13][CH2:14][S:15][CH3:16])[C:3]=1[C:4]#[N:5])(=[O:20])(=[O:19])[NH2:18]

Participants

3

Reactant 2

HCID 24499Chlorosulfamic acidHCID 66745680HCID 66745680, compound

Product 1

HCID 66746588HCID 66746588, compoundYield 66%

Procedure

Prepared as in Example 215a from 2-amino-6-(4-(methylthio)-butoxy)benzonitrile (Example 244b) and sulfamoyl chloride in 66% yield. MS 316 (MH+).

Sources & evidence

ORD record
ord-4c9f4b545c6442dfbf052a7f78610c76
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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