Diethylene Glycol Monoethyl Ether → HCID 67400146, compound

HRID 711882Notes

Reaction equation

HRID 711882 reaction equation
[CH2:1]([O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][OH:9])[CH3:2].[N+:10]([C:13]1[CH:20]=[CH:19][CH:18]=[C:17]([N+]([O-])=O)[C:14]=1[C:15]#[N:16])([O-:12])=[O:11]>>[CH2:1]([O:3][CH2:4][CH2:5][O:6][CH2:7][CH2:8][O:9][C:17]1[CH:18]=[CH:19][CH:20]=[C:13]([N+:10]([O-:12])=[O:11])[C:14]=1[C:15]#[N:16])[CH3:2]

Participants

3

Reactant 2

HCID 8146Diethylene Glycol Monoethyl EtherHCID 520718Dinitrobenzonitrile

Product 1

HCID 67400146HCID 67400146, compoundYield 66%

Procedure

Prepared as in Example 215c from 2-(2-ethoxyethoxy)ethanol and 2,6-dinitrobenzonitrile in 66% yield. MS 281 (MH+).

Sources & evidence

ORD record
ord-28dd6d978a3b4a628fdf80e0882c470a
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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