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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 711919Generated: October 26, 2026

1,9-Nonanediol → 2-(9-Hydroxynonyloxy)-6-nitrobenzonitrile

https://huagongshe.com/reaction/711919

Reaction equation

Participants

RoleNameHCIDCharge
Reactant1,9-NonanediolHCID 19835—
Reactant1,1,3,3-TetramethylguanidineHCID 66460—
Reactant1,8-Diazabicyclo(5.4.0)undec-7-eneHCID 81184—
ReactantDinitrobenzonitrileHCID 520718—
Product2-(9-Hydroxynonyloxy)-6-nitrobenzonitrileHCID 6674584430.7%

Reaction Steps

Prepared as in Example 274c (except DBU was replaced with 1,1,3,3-tetramethylguanidine) from 1,9-nonanediol and 2,6-dinitrobenzonitrile in 30.7% yield. MS 307 (MH+).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09181276B2
Source datasetuspto-grants-2015_11
ORD IDord-cb45c08645774286b14ae0252469b5ee
Source noteuspto-grants-2015_11