Dinitrobenzonitrile → HCID 66746705, compound

HRID 711925Notes

Reaction equation

HRID 711925 reaction equation
[N:1]1([CH2:6][CH2:7][OH:8])[CH:5]=[CH:4][CH:3]=[CH:2]1.[N+:9]([C:12]1[CH:19]=[CH:18][CH:17]=[C:16]([N+]([O-])=O)[C:13]=1[C:14]#[N:15])([O-:11])=[O:10]>>[N:1]1([CH2:6][CH2:7][O:8][C:16]2[CH:17]=[CH:18][CH:19]=[C:12]([N+:9]([O-:11])=[O:10])[C:13]=2[C:14]#[N:15])[CH:5]=[CH:4][CH:3]=[CH:2]1

Participants

3

Reactant 2

HCID 520718DinitrobenzonitrileHCID 109754381-(2-Hydroxyethyl)pyrrole

Product 1

HCID 66746705HCID 66746705, compoundYield 42.5%

Procedure

Prepared as in Example 166d from 2-(1H-pyrrol-1-yl)ethanol and 2,6-dinitrobenzonitrile, in 42.5% yield. MS 258 (MH+).

Sources & evidence

ORD record
ord-bdf656c332394a58844462af77f3c1bb
Source dataset
uspto-grants-2015_11
Patent number
US09181276B2

Reaction notes

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