HCID 86717540, compound → HCID 86717541, compound

Participants

Reaction Steps

A mixture of tert-butyl (3S)-3-[(6-nitrothieno[3,2-b]pyridin-7-yl)amino]piperidine-1-carboxylate (0.26 g, 0.69 mmol) and 10% palladium on carbon (80 mg) in methanol (5.0 mL) was stirred under an atmosphere of H2 (balloon) overnight. The mixture was filtered through a pad of Celite and concentrated to give 0.24 g of the desired product. LCMS calculated for C17H25N4O2S (M+H)+: m/z=349.2. Found: 349.0.

Provenance & Evidence