HRID712379

反应详情

EQUATION

反应方程式

HRID 712379 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 3-(trifluoromethyl)[1,2,4]triazolo[4,3-a]pyrazine (1.60 g) in methanol (20 mL) was added a catalytic amount of Pd/C. The suspension was stirred under H2 for 5 h, and then filtered. The filtrate was concentrated in vacuo to give a residue, which was used for next step without further purification.

WORKUP

后处理

  1. filtrationfiltered
  2. concentrationThe filtrate was concentrated in vacuo
  3. customto give a residue, which
  4. customwas used for next step without further purification