HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetrahydrofuran → HCID 131733989, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetrahydrofuran | HCID 8028 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 86730618 | HCID 86730618 | — |
| Reactant | HCID 86730621 | HCID 86730621 | — |
| Product | HCID 131733989 | HCID 131733989 | — |
Reaction Steps
The 2-methoxy-5-ethoxy-4-((tri-iso-propylsilyl)ethynyl)benzaldehyde and diethyl 2-ethoxy-4-iodo-5-methoxybenzylphosphonate can be added to a solution containing sodium hydride (NaH) dissolved in tetrahydrofuran (THF), yielding (E)-(4-(2-ethoxy-4-iodo-5-methoxystyryl)-(2-ethoxy-5-methylphenyl)ethynyl)tri-iso-propylsilane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09181287B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-d4ded3ff1d324508bd704d98c90227e1 |
| Source note | uspto-grants-2015_11 |