HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 67026145, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Nicotinoyl chloride | HCID 82604 | — |
| Reactant | 5-Fluoroisophthalonitrile | HCID 2783094 | — |
| Reactant | HCID 73855262 | HCID 73855262 | — |
| Product | HCID 67026145 | HCID 67026145 | — |
Reaction Steps
The title compound was prepared according to the procedure of Example 4B using 3-cyano-5-fluoro-N′-hydroxybenzimidamide (Prepared from 5-fluoroisophthalonitrile using the procedure described in Example 4A) and nicotinoyl chloride (Aldrich). 1H NMR (300 MHz, DMSO-d6) δ 7.77 (m, 1H), 8.2 (m, 2H), 8.4 (m, 1H), 8.6 (m, 1H), 8.9 (m, 1H), 9.4 (m, 1H) ppm; MS (DCl/NH3) m/z 267 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09186407B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-5027043716d14eaaab483bd7e80ac035 |
| Source note | uspto-grants-2015_11 |