HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Ethyl chloroformate → HCID 71811403, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Ethyl chloroformate | HCID 10928 | — |
| Edukt | 4-(8-Amino-5,6,7,8-tetrahydro-4-isoquinolinyl)benzonitrile | HCID 71811360 | — |
| Produkt | HCID 71811403 | HCID 71811403 | 39% |
Reaktionsschritte
In analogy to the procedure described for the preparation of example 3, (rac)-4-(8-amino-5,6,7,8-tetrahydroisoquinolin-4-yl)benzonitrile (example 1) was reacted with ethyl chloroformate to give the title compound as a off-white powder in 39% yield. MS: 322.2 (M+H+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09187429B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-f08f1bd5b84a459190a64ce94ede92f3 |
| Quellennotiz | uspto-grants-2015_11 |