HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzenesulfonyl chloride → HCID 86708033, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzenesulfonyl chloride | HCID 7404 | — |
| Reactant | 1,3-Benzothiazole-6-sulfonyl chloride | HCID 2795170 | — |
| Reactant | HCID 86708034 | HCID 86708034 | — |
| Product | HCID 86708033 | HCID 86708033 | 58% |
Reaction Steps
The title compound was prepared in 58% yield from intermediate 34 following the procedure described for the step 8 in scheme I corresponding to the synthesis of example 1 but using 1,3-benzothiazole-6-sulfonyl chloride instead 4-nitrobenzene sulfonyl chloride MS: m/z=898.3 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187415B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-efb9ca1c0e6f4b7d9a53c581feb8e953 |
| Source note | uspto-grants-2015_11 |