HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl formate → HCID 89874231, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl formate | HCID 74626 | — |
| Reactant | HCID 89874616 | HCID 89874616 | — |
| Product | HCID 89874231 | HCID 89874231 | 73% |
Reaction Steps
The title compound is prepared in 73% yield (90 mg, yellow oil) from 4-chloro-2-(1-(3-methyl-4-(2,2,2-trifluoroethoxy)phenyl)ethyl)-2,3-dihydro-1H-pyrrolo[3,4-c]pyridin-1-one (100 mg, 0.26 mmol, Intermediate-42, single enantiomer) and phenyl formate (64 mg, 0.52 mmol) in a similar manner to Intermediate-91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-c0158b4fa2974869b5840766e099e4b4 |
| Source note | uspto-grants-2015_11 |