HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl formate → HCID 89874683, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl formate | HCID 74626 | — |
| Reactant | HCID 89875391 | HCID 89875391 | — |
| Product | HCID 89874683 | HCID 89874683 | 70% |
Reaction Steps
The title compound is prepared in 70% yield (86 mg, yellow oil) from 4-chloro-2-(1-(3-chloro-4-(2,2-difluoroethoxy)phenyl)ethyl)-2,3-dihydro-1H-pyrrolo[3,4-c]pyridin-1-one (100 mg, 0.26 mmol, Intermediate-25, single enantiomer) and phenyl formate (63 mg, 0.52 mmol) in a similar manner to Intermediate-91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-2e06c2417f16424d86c01704c82d2e5b |
| Source note | uspto-grants-2015_11 |