HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl formate → HCID 89874926, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl formate | HCID 74626 | — |
| Reactant | HCID 89874265 | HCID 89874265 | — |
| Product | HCID 89874926 | HCID 89874926 | 68% |
Reaction Steps
The title compound is prepared in 68% yield (200 mg, pale brown solid) from 4-chloro-2-((5-(2,2-difluoroethoxy)-4-methylpyridin-2-yl)methyl)-2,3-dihydro-1H-pyrrolo[3,4-c]pyridin-1-one (240 mg, 0.68 mmol, Intermediate-69) and phenyl formate (170 mg, 1.4 mmol) in a similar manner to Intermediate-91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-19749f4082bf427283dd125be8492765 |
| Source note | uspto-grants-2015_11 |