HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl formate → HCID 89875344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl formate | HCID 74626 | — |
| Reactant | HCID 89874489 | HCID 89874489 | — |
| Product | HCID 89875344 | HCID 89875344 | 70% |
Reaction Steps
The title compound is prepared in 70% yield (130 mg, brown oil) from 4-chloro-2-(1-(5-chloro-6-(2,2,3,3-tetrafluoropropoxy)pyridin-3-yl)ethyl)-2,3-dihydro-1H-pyrrolo[3,4-c]pyridin-1-one (150 mg, 0.34 mmol, Intermediate-77, single enantiomer) and phenyl formate (84 mg, 0.69 mmol) in a similar manner to Intermediate-91.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-583c264d8a9d4c6fbe20f46da44c51b1 |
| Source note | uspto-grants-2015_11 |