HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butylsulfinamide, (R)-(+)- → HCID 89875207, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butylsulfinamide, (R)-(+)- | HCID 10964479 | — |
| Reactant | HCID 89874410 | HCID 89874410 | — |
| Product | HCID 89875207 | HCID 89875207 | 76% |
Reaction Steps
The title compound is prepared in 76% yield (2.96 g, white solid) from 1-(5-chloro-6-(3,3,3-trifluoropropoxy)pyridin-3-yl)ethanone (2.80 g, 10.5 mmol, Step-3) and (R)-2-methylpropane-2-sulfinamide (1.90 g, 15.7 mmol) in a similar manner to Step-4 of Amine-1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187475B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-a99d07e066134252bd73bc9e64e5ec43 |
| Source note | uspto-grants-2015_11 |