2-((3R,3aR,6R,6aS)-6-(tert-butyldimethylsilyloxy)hexahydrofuro[3,2-b]furan-3-yloxy)-6-chloro-5-iodo-3-((2-(tri-methylsilyl)ethoxy)methyl)-3H-imidazo[4,5-b]pyridine → HCID 178455385, compound

Participants

Reaction Steps

The title compound is prepared from 2-((3R,3aR,6R,6aS)-6-(tert-butyldimethylsilyloxy)hexahydrofuro[3,2-b]furan-3-yloxy)-6-chloro-5-iodo-3-((2-(tri-methylsilyl)ethoxy)methyl)-3H-imidazo[4,5-b]pyridine and (cis)-4-(4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)cyclohexanol following a procedure analogous to that described for Intermediate 7 Step 2. LC (method 5): tR=1.21 min; Mass spectrum (ESI+): m/z=716 [M+H]+.

Provenance & Evidence