HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl chloroformate → Benzyl 4-(methoxycarbonylamino)piperidine-1-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl chloroformate | HCID 6586 | — |
| Reactant | 4-Amino-1-N-Cbz-piperidine | HCID 17846640 | — |
| Product | Benzyl 4-(methoxycarbonylamino)piperidine-1-carboxylate | HCID 18677680 | — |
Reaction Steps
The title compound is prepared from benzyl 4-aminopiperidine-1-carboxylate and methyl chloroformate following a procedure analogous to that described for Intermediate 26 Step 1. LC (method 1): tR=0.92 min; Mass spectrum (ESI+): m/z=293 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187477B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-3e08bc7cc04f4e5abdd9a6f7d3265909 |
| Source note | uspto-grants-2015_11 |