HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 46318272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 46318296 | HCID 46318296 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 46318272 | HCID 46318272 | — |
Reaction Steps
(tert-Butoxy)-N-[1-(pyrrolidinylcarbonyl)(4-piperidyl)]carboxamide (2.0 g, 6.73 mmol) was dissolved in 40 mL dichloromethane and trifluoroacetic acid (15 mL, 201.94 mmol) were added. The reaction mixture was stirred for 4 hours. The solvent was evaporated to give the product as a light brown semi-solid, which was used directly for the next step. (2.09 g, 6.73 mmol, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09187479B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-8a4082498c5e42cfbd2877b5954d51ed |
| Source note | uspto-grants-2015_11 |