Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → (E)-methyl 3-(3-methoxyphenyl)acrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 3-Methoxycinnamic Acid | HCID 637668 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | (E)-methyl 3-(3-methoxyphenyl)acrylate | HCID 11041597 | — |
반응 단계
A mixture of (E)-3-(3-methoxyphenyl)acrylic acid (3.56 g, 20 mmol). K2CO3 (3.1 g, 22 mmol), and iodomethane (4.0 g, 28 mmol) in acetone (20 mL) was heated to 70° C. for 16 hours. The mixture was concentrated and partitioned between water and ethyl acetate to afford the crude title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US09187483B2 |
| 출처 데이터셋 | uspto-grants-2015_11 |
| ORD ID | ord-d04f77836ff34219b92b4a1192de63a6 |
| 출처 메모 | uspto-grants-2015_11 |