HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
N-(tert-butoxycarbonyl)glycine → N-Boc-glycyl-L-proline benzyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | N-(tert-butoxycarbonyl)glycine | HCID 78288 | — |
| Edukt | Proline benzyl ester hydrochloride | HCID 2733413 | — |
| Edukt | (S,R)-1-(2-tert-butoxycarbonylamino-2-phenylacetyl)-pyrrolidine-2-carboxylic acid benzyl ester | HCID 15288611 | — |
| Produkt | N-Boc-glycyl-L-proline benzyl ester | HCID 13152016 | — |
Reaktionsschritte
Compound 26 was synthesized from N-Boc-glycine and L-proline benzyl ester hydrochloride, following the procedure as described for compound 2a, as a white crystallized solid. MS (ESI, EI+) m/z=363 (MH+).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US09187496B2 |
| Quelldatensatz | uspto-grants-2015_11 |
| ORD ID | ord-041d1bc54f624b73875af38c6f667297 |
| Quellennotiz | uspto-grants-2015_11 |