HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methacrylic Acid → Solanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methacrylic Acid | HCID 4093 | — |
| Reactant | Ethylene glycol dimethacrylate | HCID 7355 | — |
| Reactant | HCID 89183541 | HCID 89183541 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Solanone | HCID 6451337 | — |
Reaction Steps
Methacrylic acid (3 mol percent), EGDMA (95 mol percent), and 5-isopropyl-8-methylnonan-2-one (2 mol percent) are combined in toluene. 2,2-Azobisisobutyronitrile (AIBN) is added as an initiator. The reaction flask is degassed, purged with dry nitrogen, and sealed. The solution is irradiated with a UV lamp (365 nm) to activate the AIBN and initiate the polymerization reaction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09192193B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-b5ac5cf49dcf4455a1dc12b61b82caa9 |
| Source note | uspto-grants-2015_11 |