HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → 1-(2-methylpropyl)-2,4-dihydro-1H-3,1-benzoxazine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | Isobutyl iodide | HCID 10556 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Product | 1-(2-methylpropyl)-2,4-dihydro-1H-3,1-benzoxazine-2,4-dione | HCID 3578689 | — |
Reaction Steps
Reagents: Isatoic anhydride (6.13 mmols, 1 g); Sodium hydride (9.2 mmols, 0.22 g); isobutyl iodide (18 mmols, 3.4 g). Yield: 0.6 g (46%), white solid, m.p.=85° C.-86° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193688B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-483b9ba0cdbd4818ae99262142fa6688 |
| Source note | uspto-grants-2015_11 |