HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → N-(cyclopropylmethyl)isatoic anhydride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | Bromomethylcyclopropane | HCID 81503 | — |
| Product | N-(cyclopropylmethyl)isatoic anhydride | HCID 11672969 | — |
Reaction Steps
Reagents: Isatoic anhydride (4.9 mmols, 0.8 g); Sodium hydride (5.9 mmols, 0.14 g); Cyclopropylmethyl bromide (5.9 mmols, 0.8 g). Yield: 0.53 g (50%), light brown solid, m.p.=122° C.-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193688B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-4bce59b6273d4bfaa8661e80b17ced94 |
| Source note | uspto-grants-2015_11 |