Benzoyl chloride, 3-chloro- → HCID 2276416, compound

HRID 716736Notes

Reaction equation

HRID 716736 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5](Cl)=[O:6].[C:11]([O:15][C:16]([CH3:19])([CH3:18])[CH3:17])(=[O:14])[NH:12][NH2:13]>>[Cl:1][C:2]1[CH:3]=[C:4]([CH:8]=[CH:9][CH:10]=1)[C:5]([NH:13][NH:12][C:11]([O:15][C:16]([CH3:19])([CH3:18])[CH3:17])=[O:14])=[O:6]

Participants

3

Reactant 2

HCID 69252Benzoyl chloride, 3-chloro-HCID 70091tert-Butyl carbazate

Product 1

HCID 2276416HCID 2276416, compound

Procedure

The title compound (4.41 g, colorless powder) was synthesized from 3-chlorobenzoyl chloride (2 mL) and tert-butyl carbazate (2.49 g), as in Reference Example P-Q1b.

Sources & evidence

ORD record
ord-d7f1482402ba4498bcdf656297be7c79
Source dataset
uspto-grants-2015_11
Patent number
US09193695B2

Reaction notes

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