Acetic Acid → HCID 90269079, compound

Participants

Reaction Steps

0.5 mmol of 4-((3-phenyl-isoxazol-5-yl)-methoxy-)-quinazoline was added to a 50 mL single-necked round-bottom flask containing 10 mL of dry dichloromethane. 2 mL of glacial acetic acid was added under stirring. The mixture was stirred for 1-2 hours at 30-40, cooled down, and then crystallized under refrigeration, filtered and dried under vacuum to afford 4-((3-phenyl-isoxazol-5-yl)-methoxy-)-quinazoline acetate as a colorless solid in 58% yield.

Provenance & Evidence