HuagongsheHuagongshe Chemistry Print Report · For research reference only
tert-Butyl (4-bromo-2-nitrophenyl)carbamate → (2-Amino-4-bromo-phenyl)-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | tert-Butyl (4-bromo-2-nitrophenyl)carbamate | HCID 52904808 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | (2-Amino-4-bromo-phenyl)-carbamic acid tert-butyl ester | HCID 68693978 | — |
Reaction Steps
The title compound was prepared from the tert-butyl 4-bromo-2-nitrophenylcarbamate (Example A1; 3 mmol) by reduction with zinc according to the general procedure B. Obtained as a yellow solid (58%), MS (EI) 287 [(M+1)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193710B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-f6f1a4bb03d74a1483edf151edd51b00 |
| Source note | uspto-grants-2015_11 |