HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tert-butyl (4-iodo-2-nitrophenyl)carbamate → (2-Amino-4-iodo-phenyl)-carbamic acid tert-butyl ester
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tert-butyl (4-iodo-2-nitrophenyl)carbamate | HCID 23554339 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | (2-Amino-4-iodo-phenyl)-carbamic acid tert-butyl ester | HCID 69592774 | — |
Reaction Steps
The title compound was prepared from the tert-butyl 4-iodo-2-nitrophenylcarbamate (Example A3; 3 mmol) by reduction with zinc according to the general procedure B. Obtained as a yellow solid (44%), MS (EI) 335 [(M+1)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193710B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-9289f726bb2346529edd0189d64d88b5 |
| Source note | uspto-grants-2015_11 |