HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-[(tert-butoxy)carbonylamino]-3-nitrobenzoate → Methyl 3-amino-4-[(tert-butoxycarbonyl)amino]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-[(tert-butoxy)carbonylamino]-3-nitrobenzoate | HCID 22988663 | — |
| Catalyst | Zinc | HCID 23994 | — |
| Product | Methyl 3-amino-4-[(tert-butoxycarbonyl)amino]benzoate | HCID 18621647 | — |
Reaction Steps
The title compound was prepared from the methyl 3-nitro-4-((tert-butoxycarbonyl)amino)benzoate (Example A4; 3 mmol) by reduction with zinc according to the general procedure B. Obtained as a yellow solid (71%), MS (EI) 267 [(M+1)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193710B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-db3a3384843c452ab6abcce6e2440a41 |
| Source note | uspto-grants-2015_11 |