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HRID717524

反应详情

EQUATION

反应方程式

HRID 717524 的结构方程式

REACTANTS

反应物

1
反应SMILES：CC(C)(C)OC(=O)Nc1ccc(Cl)cc1[N+](=O)[O-]
HCID53980145

1,1-Dimethylethyl N-(4-chloro-2-nitrophenyl)carbamate

C11H13ClN2O4

PRODUCTS

产物

1
反应SMILES：CC(C)(C)OC(=O)Nc1ccc(Cl)cc1N
HCID57456272

1,1-Dimethylethyl N-(2-amino-4-chlorophenyl)carbamate

C11H15ClN2O2

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：[Zn]
催化剂HCID23994

Zinc

Zn

PROCEDURE

实验过程

The title compound was prepared from the tert-butyl 4-chloro-2-nitrophenylcarbamate (Example A5; 3 mmol) by reduction with zinc according to the general procedure B. Obtained as a yellow solid (85%), MS (EI) 243 [(M+1)+].