HCID 65142788, compound → 371158-46-2

HRID 717526Notes

Reaction equation

HRID 717526 reaction equation
[CH3:1][C:2]1[C:7]([CH3:8])=[CH:6][C:5]([NH:9][C:10](=[O:16])[O:11][C:12]([CH3:15])([CH3:14])[CH3:13])=[C:4]([N+:17]([O-])=O)[CH:3]=1>[Zn]>[NH2:17][C:4]1[CH:3]=[C:2]([CH3:1])[C:7]([CH3:8])=[CH:6][C:5]=1[NH:9][C:10](=[O:16])[O:11][C:12]([CH3:14])([CH3:13])[CH3:15]

Participants

3

Reactant 1

HCID 65142788HCID 65142788, compound

Product 1

HCID 11447711371158-46-2

Reagents, catalysts & solvents 1

HCID 23994ZincCatalyst

Procedure

The title compound was prepared from the tert-butyl 4,5-dimethyl-2-nitrophenylcarbamate (Example A7; 3 mmol) by reduction with zinc according to the general procedure B. Obtained as a yellow solid (56%), MS (EI) 237 [(M+1)+].

Sources & evidence

ORD record
ord-840fd4c375ce46b3b117d691951e5744
Source dataset
uspto-grants-2015_11
Patent number
US09193710B2

Reaction notes

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