HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Amino-4-bromo-phenyl)-carbamic acid tert-butyl ester → HCID 89421713, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Amino-4-bromo-phenyl)-carbamic acid tert-butyl ester | HCID 68693978 | — |
| Reactant | HCID 71281624 | HCID 71281624 | — |
| Product | HCID 89421713 | HCID 89421713 | — |
Reaction Steps
The title compound was prepared from the reaction of tert-butyl 2-amino-4-bromophenylcarbamate (Example B1; 1 mmol) and tert-butyl 3-oxo-3-(pyrazin-2-yl)propanoate (Example C3; 1 mmol) according to the general procedure D. Obtained as a yellow solid (81%), MS (EI) 435 [(M+1)+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193710B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-9935557142ad4fa3b3c44d8a0f3086c4 |
| Source note | uspto-grants-2015_11 |