HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66614892, compound → HCID 58571278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66614892 | HCID 66614892 | — |
| Reactant | Ethyl 3-(3-(4-octylphenyl)ureido)propanoate | HCID 66615004 | — |
| Product | HCID 58571278 | HCID 58571278 | 84% |
Reaction Steps
When the product of Step D was substituted for ethyl 3-(3-(4-octylphenyl)ureido)propanoate in Example 11, Step B, the identical process afforded the title compound in 84% yield, as a colourless solid. 1H-NMR (CDCl3) 7.68 (d, 1H, J=8.7 Hz); 6.94 (m, 2H); 5.24 (t, 1H, J=5.9 Hz); 3.86 (t, 2H, J=8.7 Hz); 3.58 (q, 2H, J=5.9 Hz); 3.11 (t, 2H, J=8.5 Hz); 2.67 (t, 2H, J=5.8 Hz); 2.5 (t, 2H, J=8 Hz); 1.54 (m, 2H); 1.25 (m, 10H); 0.86 (t, 3H, J=6.8 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193716B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-b44ff17a2d0148088d19c36f7da0258c |
| Source note | uspto-grants-2015_11 |