HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 717831Generated: November 3, 2026
Hydrogen Peroxide → HCID 58515933, compound
https://huagongshe.com/reaction/717831
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Methyl 2,5-Dichloronicotinate | HCID 2764318 | — |
| Product | HCID 58515933 | HCID 58515933 | 99% |
Reaction Steps
A solution of methyl 2,5-dichloronicotinate (15 g, 73 mmol), trifluoroacetic acid (91 mL) and 30% aqueous hydrogen peroxide solution (15 mL) were stirred and heated at 70° C. for 1 hour. Evaporation and purification by flash column chromatography using ethyl acetate in hexanes (0-100%) gave the desired product (16 g, 99%). LCMS calculated for C7H6Cl2NO3 (M+H)+: m/z=222.0. found: 221.8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09193721B2 |
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| Source dataset | uspto-grants-2015_11 |
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| ORD ID | ord-eb3fe48cfd20478b97e96c017f9c91e4 |
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| Source note | uspto-grants-2015_11 |
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