Dichloromethane → HCID 178463545, compound

Participants

Reaction Steps

To tert-butyl 4-{8-chloro-6-[1-(9H-purin-6-ylamino)ethyl]imidazo[1,5-a]pyridin-5-yl}piperazine-1-carboxylate (8.0 mg, 0.016 mmol) in methylene chloride (0.5 mL, 8 mmol), 4.0 M hydrogen chloride in 1,4-dioxane (1.0 mL, 4.0 mmol) was added. The mixture was stirred for 15 minutes. Evaporation gave the desired compound (7.5 mg, 99%). LCMS calculated for C18H21ClN9 (M+H)+: m/z=398.2. found: 397.9.

Provenance & Evidence