HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl 4-aminobenzoate → HCID 7741301, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl 4-aminobenzoate | HCID 12082 | — |
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | Cyclopentylacetyl chloride | HCID 3485182 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 7741301 | HCID 7741301 | — |
Reaction Steps
A solution of methyl 4-aminobenzoate (0.25 g, 1.654 mmol) in tetrahydrofuran (8.27 ml) was treated with diisopropylethylamine (0.433 ml, 2.481 mmol) and 2-cyclopentylacetyl chloride (0.279 g, 1.902 mmol) and the reaction mixture was stirred at ambient temperature for 2 hours. Concentration and normal phase chromatography provided the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09193723B2 |
| Source dataset | uspto-grants-2015_11 |
| ORD ID | ord-097b999c3edb4258bc889d5e263f5da9 |
| Source note | uspto-grants-2015_11 |