Hydrochloric Acid → HCID 67007111, compound

Participants

Reaction Steps

To a saturated mixture of HCl (gas) and nitromethane (25 mL) was added title compound 247 (0.85 g, 2.264 mmol). The clear solution was stirred 2 h then concentrated. The beige residue was triturated with ether overnight and filtered to afford title compound 248 (315 mg, 39%) as a beige solid. LRMS (ESI): (calc.) 319.13. (found) 320.3 (MH)+.

Provenance & Evidence