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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 718526Generated: October 31, 2026

Phenethyltriphenylphosphonium bromide → HCID 86702772, compound

https://huagongshe.com/reaction/718526

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenethyltriphenylphosphonium bromideHCID 10863251—
ReactantHCID 57429401HCID 57429401—
ReactantButyllithiumHCID 178418339—
ProductHCID 86702772HCID 8670277261.1%

Reaction Steps

Starting from phenethyltriphenylphosphonium bromide (2.60 g, 5.81 mmol, 1.0 equiv.), n-BuLi (1.3 M in hexanes, 4.5 mL, 5.81 mmol, 1.0 equiv.) and 3-(3-tert-butylcyclohexyl)propanal (1.45 g, 7.39 mmol, 1.3 equiv.), 1.01 g (61%) of the title compound as a colorless oil was obtained after purification by flash chromatography on SiO2 (cyclohexane).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09193935B2
Source datasetuspto-grants-2015_11
ORD IDord-f660562352cb43eeadb1fe4efb3dec68
Source noteuspto-grants-2015_11