2-Quinolinecarboxaldehyde → HCID 117732478, compound

Participants

Reaction Steps

Using the procedure described in Example 21, Step C, the title compound was prepared from Compound 23b and 2-quinolinecarbaldehyde. 1H-NMR (400 MHz, CDCl3) δ (ppm): 8.66 (d, J=2.2 Hz, 1H), 8.09 (d, J=8.3 Hz, 1H), 7.97-8.07 (m, 2H), 7.89 (d, J=5.6 Hz, 1H), 7.79 (d, J=8.1 Hz, 1H), 7.70 (ddd, J=8.4, 6.9, 1.3 Hz, 1H), 7.46-7.56 (m, 2H), 6.81 (d, J=9.0 Hz, 1H), 6.03 (d, J=5.6 Hz, 1H), 5.30 (t, J=5.3 Hz, 1H), 4.91 (d, J=5.4 Hz, 2H), 3.81 (s, 8H), 3.49-3.69 (m, 8H), 1.50 (s, 9H). Mass Spectrum (LCMS, ESI pos.) Calcd. For C34H39N9O3: 622.3 (M+H). Found: 622.3.

Provenance & Evidence