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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 718651Generated: October 29, 2026

2-Chloromethyl 2-(trimethylsilyl)ethyl ether → HCID 123860259, compound

https://huagongshe.com/reaction/718651

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-Chloromethyl 2-(trimethylsilyl)ethyl etherHCID 2724271—
Reactant1-(4-Bromophenyl)-1,2-dihydro-3H-1,2,4-triazol-3-oneHCID 23434192—
ProductHCID 123860259HCID 123860259—

Reaction Steps

Compound 52b (30.0 g, 125 mmol) was treated with SEMCl as described in Example 51, Step C to obtain compound 52c as a white solid. Mass Spectrum (LCMS, ESI pos.): Calcd. for C14H20BrN3O2S: 370.1 (M+H). Found 370.2.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09193736B2
Source datasetuspto-grants-2015_11
ORD IDord-23611709c9514951bceab340e04f0642
Source noteuspto-grants-2015_11