HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Chloro-phenyl)-pentane-1,2-diamine → HCID 178440009, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Chloro-phenyl)-pentane-1,2-diamine | HCID 21896886 | — |
| Reactant | Ethyl 2-isopropoxy-4-methoxybenzimidate hydrochloride | HCID 21896893 | — |
| Reactant | 5-(4-chloro-phenyl)-4-cyclopentylmethyl-2-(2-ethoxy-4-methoxy-phenyl)-4,5-dihydro-1H-imidazole | HCID 178467016 | — |
| Product | HCID 178440009 | HCID 178440009 | — |
Reaction Steps
5-(4-Chloro-phenyl)-2-(2-isopropoxy-4-methoxy-phenyl)-4-propyl-4,5-dihydro-1H-imidazole was prepared from 1-(4-chloro-phenyl)-pentane-1,2-diamine and ethyl 2-isopropoxy-4-methoxy-benzimidate hydrochloride in an analogous manner as described for the preparation of 5-(4-chloro-phenyl)-4-cyclopentylmethyl-2-(2-ethoxy-4-methoxy-phenyl)-4,5-dihydro-1H-imidazole (Example 9). HR-MS (ES, m/z) observed 387.1840, calculated for C22H28N2O2Cl [(M+H)+]387.1834.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132421B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-1f3cec03bd344270b875af9c9fcfea8a |
| Source note | uspto-grants-2006_11 |