Pyridine → HCID 10135678, compound

Participants

Reaction Steps

To a solution of 4-amino-benzo[a]phenazine-11-carboxylic acid (2-dimethylamino-ethyl)-amide (20 mg) in tetrahydrofuran (5 mL) was added pyridine (0.1 mL) and acetyl chloride (20 μL). After stirring for 1 hour the reaction mixture was extracted into ethyl acetate, washed with sodium bicarbonate solution, dried (MgSO4) and the solvent removed in vacuo The residue was triturated with ether to yield the title compound as a yellow solid (10 mg).

Provenance & Evidence