m-Anisoyl chloride → HCID 178489094, compound

HRID 719271Notes

Reaction equation

HRID 719271 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[NH:13][N:12]=[C:11]([CH3:14])[C:10]=2[NH2:15])=[CH:5][CH:4]=1.[CH3:16][O:17][C:18]1[CH:19]=[C:20]([CH:24]=[CH:25][CH:26]=1)[C:21](Cl)=[O:22]>>[CH3:16][O:17][C:18]1[CH:19]=[C:20]([CH:24]=[CH:25][CH:26]=1)[C:21]([NH:15][C:10]1[C:11]([CH3:14])=[N:12][NH:13][C:9]=1[C:6]1[CH:5]=[CH:4][C:3]([O:2][CH3:1])=[CH:8][CH:7]=1)=[O:22]

Participants

3

Reactant 2

HCID 74374m-Anisoyl chlorideHCID 178489089HCID 178489089, compound

Product 1

HCID 178489094HCID 178489094, compound

Procedure

The preparation took place in analogy with Example 15a), starting with 300 mg of 5-(4-methoxyphenyl)-3-methyl-1H-pyrazol-4-ylamine (50) and 277 mg of 3-methoxybenzoyl chloride. The following was obtained: 59.

Workup

  1. customThe following was obtained

Sources & evidence

ORD record
ord-9c9c3e079505408e9dbaf9e3c5bf8443
Source dataset
uspto-grants-2006_11
Patent number
US07132428B2

Reaction notes

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