HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzoyl chloride → HCID 178434586, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | 3-[3-(Dimethylamino)phenyl]-5-methyl-1H-pyrazol-4-amine | HCID 178434585 | — |
| Product | HCID 178434586 | HCID 178434586 | — |
Reaction Steps
The preparation was carried out as in Example 22A, using 460 mg of benzoyl chloride and 700 mg of 4-amino-5-(3-dimethylamino-phenyl)-3-methylpyrazole, except the reaction mixture was stirred for 16 h and the residue was purified by MPLC (ethyl acetate as eluant) to give the title compound as a tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132428B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-db322e4b1f3d4434ad7439abe93c5491 |
| Source note | uspto-grants-2006_11 |