HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(2-Chlorophenyl)-1,3-thiazol-2-amine → 2,4-Dichloro-N-[4-(2-chlorophenyl)-1,3-thiazol-2-yl]-6-methylbenzenesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(2-Chlorophenyl)-1,3-thiazol-2-amine | HCID 224764 | — |
| Reactant | 2,4-Dichloro-6-methylbenzenesulfonyl chloride | HCID 2801387 | — |
| Product | 2,4-Dichloro-N-[4-(2-chlorophenyl)-1,3-thiazol-2-yl]-6-methylbenzenesulfonamide | HCID 10203190 | — |
Reaction Steps
The title compound was prepared from 4-(2-chlorophenyl)-1,3-thiazol-2-amine and 2,4 -dichloro-6-methylbenzenesulfonyl chloride as described in the synthetic METHOD B to give a white solid (40.3 mg) with purity >90%. MS (pos) m/z 435.0, 437.0.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-f0bf3e2c4d634264b7f8118ef1ad0c26 |
| Source note | uspto-grants-2006_11 |