HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2,5-difluorobenzenesulfonyl Chloride → HCID 11167349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2,5-difluorobenzenesulfonyl Chloride | HCID 574590 | — |
| Reactant | 4-(3-Chloro-2-thienyl)-1,3-thiazol-2-amine | HCID 1488441 | — |
| Product | HCID 11167349 | HCID 11167349 | — |
Reaction Steps
The title compound was prepared 4-(3-chloro-2-thienyl)-1,3-thiazol-2-amine (59 mg) and 4-bromo-2,5-difluorobenzenesulfonyl chloride (79 mg) as described in the synthetic METHOD B to give a white solid (22.3 mg) with purity >90%: MS (pos) m/z 471.2, 473.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132436B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-88a55cc7fe7b480da9407c9be3f70ed1 |
| Source note | uspto-grants-2006_11 |