HRID719362

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID36904

2,3,4-Trichlorobenzenesulfonyl chloride

C6H2Cl4O2S

HCID1478576

4-[2-Chloro-4-(4-chlorophenoxy)phenyl]-2-thiazolamine

C15H10Cl2N2OS

PRODUCTS

生成物

结构：O=S(=O)(Nc1nc(-c2ccc(Oc3ccc(Cl)cc3)cc2Cl)cs1)c1ccc(Cl)c(Cl)c1Cl

HCID11250172

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 4-[2-chloro-4-(4-chlorophenoxy)phenyl]-1,3-thiazol-2-amine (91 mg) and 2,3,4-trichlorobenzenesulfonyl chloride (76 mg) as described in the synthetic METHOD B to give a white solid (49.2 mg) with purity >90%: MS (pos) m/z 579.1, 581.1, 583.1; MS (neg) m/z 577.5, 579.5, 581.5.