HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 21897138, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 6-chloro-N-(3-chloro-4-methoxyphenyl)-N'-cycloheptyl-[1,3,5]triazine-2,4-diamine | HCID 21897021 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21897138 | HCID 21897138 | — |
Reaction Steps
To 6-chloro-N-(3-chloro-4-methoxyphenyl)-N′-cycloheptyl-[1,3,5]triazine-2,4-diamine (5 g) dissolved in methanol was added K2CO3 (3.2 g) and refluxed for about 6–8 h. TLC was monitored. After the completion of the reaction, the reaction mass was filtered through vacuum and the filtrate was evaporated to yield the title compound. (Wt. 4.7 g Y: 95%)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07132423B2 |
| Source dataset | uspto-grants-2006_11 |
| ORD ID | ord-110603176c904dddb3bf30da5e2fa919 |
| Source note | uspto-grants-2006_11 |